600 MHz FT-NMR (Solid) | 600 MHz 고체상 핵자기 공명 분광기
| 연구실/분야 | |||
|---|---|---|---|
| 모델명 | AVANCE NEO + VNMRS600 | ||
| 제조사 | Bruker | ||
| 담당자 | 한선필 | ||
| 연락처 | 052-217-4174 / okno1234@unist.ac.kr | ||
| 예약 가능여부 | 가능 | ||
| 예약단위 | 10min | 1일최대예약시간 | 24hr |
| 예약Open(~일 전) | 5일전 | 예약취소불가(~일 전) | 1시간전 |
| 장비위치 | 102동 B119호 | ||
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Description
고체상핵자기공명 분광기로서 Varian 600 MHz Magnet + Bruker AVANCE NEO + 3.2mm CP-MAS probe로 업그레이드(2025.11.03)
NMR is a technique for determining the structure of most organic and some inorganic molecules. NMR studies a magnetic nucleus by aligning it with a very powerful external magnetic field and disturbing this alignment using an electromagnetic field. Different atoms within a molecule resonate at different frequencies at a given field strength.
https://ucrf.unist.ac.kr/en/category/data/technical-library/
1) Varian 600 MHz FT-NMR Operation Manual
2) DOSY NMR Manual
3) 2D NMR Manual
4) SOP of Bruker 400 MHz FT-NMR
https://ubts.co.kr/
NMR 이론 및 실습관련 동영상 교육자료 (NMR Theory and Practice video)
- 이론, 장비사용법, Mnova processing 등 -
Specifications
• Premium shielded 14.09 T (600 MHz) magnet
• 2 channel console
Ch1: 500 Watt
Ch2: 500 Watt
• Available probe
- 3.2 mm CP-MAS probe (Max spinning rate = 24 kHz)
Ch1: 1H, 19F
Ch2: 15N ~ 31P
Spinning rate: 1.8~24 kHz (Max: 24 kHz)
Sample amount: ~ 200 mg (fine powder) or KBr mixture
Temperature: -150C - 150C
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Applications
• Structural elucidation of chemicals
• Structural determination of biomolecules (DNA, RNA, proteins, peptides, etc.)
• Study of dynamic process
• Drug design
Detectable nuclei: 1H, 7Li, 9Be, 11B, 13C 17O, 19F, 23Na, 27Al, 29Si, 31P, 35Cl, 119Sn etc